HRID1665290

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID69252

Benzoyl chloride, 3-chloro-

C7H4Cl2O

HCID57661820

Spiro[naphtho[1,2-b]-1,4-oxathiin-2(3H),4′-piperidine]-5,6-dione

C16H15NO3S

PRODUCTS

生成物

结构：O=C1C(=O)c2ccccc2C2=C1SCC1(CCN(C(=O)c3cccc(Cl)c3)CC1)O2

HCID23654703

未命名化合物

PROCEDURE

实验过程

Compound 55 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 3-chlorobenzoyl chloride and conditions outlined in procedure N. M.p.=155-158° C.; 300 MHz 1H NMR (DMSO-d6) δ 7.89 (m, 2H), 7.69 (t, 1H), 7.52 (m, 4H), 7.40 (m, 1H), 4.40 (m, 1H), 3.50 (brm, 2H), 3.24 (m, 1H), 3.11 (s, 2H), 2.08 (m, 1H), 1.90 (m, 3H); LCMS: 440 [M+H].