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HRID1665296

反应详情

EQUATION

反应方程式

HRID 1665296 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)C=Cc1ccccc1Cl
HCID2737382

未命名化合物

结构：O=C1C(=O)c2ccccc2C2=C1SCC1(CCNCC1)O2
HCID57661820

Spiro[naphtho[1,2-b]-1,4-oxathiin-2(3H),4′-piperidine]-5,6-dione

C16H15NO3S

PRODUCTS

生成物

1
结构：O=C1C(=O)c2ccccc2C2=C1SCC1(CCN(C(=O)/C=C/c3ccccc3Cl)CC1)O2
HCID57661865

未命名化合物

PROCEDURE

实验过程

Compound 61 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 2-chlorocinnamoyl chloride and conditions outlined in procedure N. M.p.=110-115° C.; 300 MHz 1H NMR (DMSO) δ 8.0-7.75 (m, 5H), 7.6-7.4 (m, 3H), 7.4-7.25 (m, 1H), 7.2-7.1 (m, 1H), 4.5-4.35 (m, 1H), 3.45-3.05 (m, 5H), 2.25-1.7 (m, 4H); LCMS: 466 [M+H].