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HRID1665312

反应详情

EQUATION

反应方程式

HRID 1665312 的结构方程式

REACTANTS

反应物

2
结构：Cc1nn(C)c(C)c1S(=O)(=O)Cl
HCID2737340

1,3,5-trimethyl-1H-pyrazole-4-sulfonyl chloride

C6H9ClN2O2S

结构：O=C1C(=O)c2ccccc2C2=C1SCC1(CCNCC1)O2
HCID57661820

Spiro[naphtho[1,2-b]-1,4-oxathiin-2(3H),4′-piperidine]-5,6-dione

C16H15NO3S

PRODUCTS

生成物

1
结构：Cc1nn(C)c(C)c1S(=O)(=O)N1CCC2(CC1)CSC1=C(O2)c2ccccc2C(=O)C1=O
HCID57661857

未命名化合物

PROCEDURE

实验过程

Compound 80 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 1,3,5-trimethyl-1H-pyrazole-4-sulfonyl chloride and conditions outlined in procedure P. M.p.=273-275° C.; 400 MHz 1H NMR (DMSO-d6) δ: 7.88-7.85 (m, 1H), 7.64-7.58 (m, 1H), 7.56-7.52 (m, 1H), 7.32-7.29 (m, 1H), 3.72 (s, 3H), 3.50-3.44 (m, 2H), 3.09 (s, 2H), 2.71-2.65 (m, 2H), 2.38 (s, 3H), 2.22 (s, 3H), 2.11-2.05 (m, 2H), 1.91-1.82 (m, 2H); LCMS: 474 [M+H].