1-Bromodecane → HCID 57661931, compound

Participants

Reaction Steps

Compound 128 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 1-bromodecane and conditions outlined in procedure V. M.p.=110-111° C.; 400 MHz 1H NMR (CDCl3) δ 8.06 (d, J=1.2 Hz, 1H), 7.8-7.75 (m, 1H), 7.75-7.6 (m, 1H), 7.53-7.43 (m, 1H), 2.93 (s, 2H) 2.85-2.75 (m, 2H), 2.5-2.35 (m, 4H), 2.2-2.05 (m, 2H), 1.95-1.8 (m, 2H), 1.6-1.43 (m, 2H), 1.4-1.18 (m, 14H), 0.9-0.8 (m, 3H); LCMS: 442 [M+H].

Provenance & Evidence