Allyl bromide → HCID 57661846, compound

Participants

Reaction Steps

Compound 131 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 3-bromoprop-1-ene and conditions outlined in procedure V. M.p.=166-168° C.; 400 MHz 1H NMR (DMSO-d6) δ: 7.9 (d, 1H), 7.75 (s, 2H), 7.55 (s, 1H), 5.8 (m, 1H), 5.2-5.1 (m, 2H), 3.1 (s, 2H), 3.0 (d, 2H), 2.7 (d, 2H), 2.3 (t, 2H), 1.95 (d, 2H), 1.8 (t, 2H); LCMS: 328 [M+H].

Provenance & Evidence