3-Bromocyclohexene → HCID 57662040, compound

HRID 1665333Notes

Reaction equation

HRID 1665333 reaction equation
[NH:1]1[CH2:6][CH2:5][C:4]2([O:11][C:10]3[C:12]4[C:17]([C:18](=[O:21])[C:19](=[O:20])[C:9]=3[S:8][CH2:7]2)=[CH:16][CH:15]=[CH:14][CH:13]=4)[CH2:3][CH2:2]1.Br[CH:23]1[CH2:28][CH2:27][CH2:26][CH:25]=[CH:24]1>>[CH:28]1([N:1]2[CH2:2][CH2:3][C:4]3([O:11][C:10]4[C:12]5[C:17]([C:18](=[O:21])[C:19](=[O:20])[C:9]=4[S:8][CH2:7]3)=[CH:16][CH:15]=[CH:14][CH:13]=5)[CH2:5][CH2:6]2)[CH2:27][CH2:26][CH2:25][CH:24]=[CH:23]1

Participants

3

Reactant 2

HCID 1370573-BromocyclohexeneHCID 57661820Spiro[naphtho[1,2-b][1,4]oxathiine-2,4'-piperidine]-5,6-dione

Product 1

HCID 57662040HCID 57662040, compound

Procedure

Compound 135 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 3-bromocyclohexene and conditions outlined in procedure V. LCMS: 382 [M+H]; Rt=0.94 min.

Sources & evidence

ORD record
ord-90d97deee924496991b5d42cc6528e23
Source dataset
uspto-grants-2011_10
Patent number
US08039503B2

Reaction notes

Loading…