(1-Bromoethyl)benzene → HCID 57661962, compound

HRID 1665335Notes

Reaction equation

HRID 1665335 reaction equation
[NH:1]1[CH2:6][CH2:5][C:4]2([O:11][C:10]3[C:12]4[C:17]([C:18](=[O:21])[C:19](=[O:20])[C:9]=3[S:8][CH2:7]2)=[CH:16][CH:15]=[CH:14][CH:13]=4)[CH2:3][CH2:2]1.Br[CH:23]([C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1)[CH3:24]>>[C:25]1([CH:23]([N:1]2[CH2:2][CH2:3][C:4]3([O:11][C:10]4[C:12]5[C:17]([C:18](=[O:21])[C:19](=[O:20])[C:9]=4[S:8][CH2:7]3)=[CH:16][CH:15]=[CH:14][CH:13]=5)[CH2:5][CH2:6]2)[CH3:24])[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1

Participants

3

Reactant 2

HCID 11454(1-Bromoethyl)benzeneHCID 57661820Spiro[naphtho[1,2-b][1,4]oxathiine-2,4'-piperidine]-5,6-dione

Product 1

HCID 57661962HCID 57661962, compound

Procedure

Compound 137 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, (1-bromoethyl)benzene and conditions outlined in procedure V. LCMS: 406 [M+H]; Rt=0.96 min.

Sources & evidence

ORD record
ord-465142aaf25a4123908b6c33a2df5384
Source dataset
uspto-grants-2011_10
Patent number
US08039503B2

Reaction notes

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