HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, (2-bromoethoxy)- → 1'-(2-Phenoxyethyl)spiro[naphtho[1,2-b][1,4]oxathiine-2,4'-piperidine]-5,6-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, (2-bromoethoxy)- | HCID 68526 | — |
| Reactant | Spiro[naphtho[1,2-b][1,4]oxathiine-2,4'-piperidine]-5,6-dione | HCID 57661820 | — |
| Product | 1'-(2-Phenoxyethyl)spiro[naphtho[1,2-b][1,4]oxathiine-2,4'-piperidine]-5,6-dione | HCID 57661992 | — |
Reaction Steps
Compound 140 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, (2-bromoethoxy)benzene and conditions outlined in procedure V. LCMS: 422 [M+H]; Rt=1.01 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039503B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-3a8f543f0f4846ae8b7b66fde5bbb4db |
| Source note | uspto-grants-2011_10 |