HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Oxabicyclo[3.1.0]hexane → HCID 57661834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Oxabicyclo[3.1.0]hexane | HCID 9244 | — |
| Reactant | Spiro[naphtho[1,2-b][1,4]oxathiine-2,4'-piperidine]-5,6-dione | HCID 57661820 | — |
| Product | HCID 57661834 | HCID 57661834 | — |
Reaction Steps
Compound 161 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 6-oxabicyclo[3.1.0]hexane and conditions outlined in procedure X. M.p.=110-113° C.; 400 MHz 1H NMR (CDCl3) δ: 8.05 (d, 1H), 7.75 (d, 1H), 7.65 (t, 1H), 7.5 (t, 1H), 4.1 (m, 1H), 3.1 (d, 1H), 2.95 (s, 1H), 2.9 (d, 1H), 2.7-2.5 (m, 3H), 2.2-1.85 (m, 8H), 1.8-1.5 (m, 4H); LCMS: 386 [M+H].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08039503B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-e3c8a3c090e240869bf7c081242a0dfd |
| Source note | uspto-grants-2011_10 |