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HRID1665366

反应详情

EQUATION

反应方程式

HRID 1665366 的结构方程式

REACTANTS

反应物

2
结构：CC(C)OCC1CO1
HCID19920

Isopropyl glycidyl ether

C6H12O2

结构：O=C1C(=O)c2ccccc2C2=C1SCC1(CCNCC1)O2
HCID57661820

Spiro[naphtho[1,2-b]-1,4-oxathiin-2(3H),4′-piperidine]-5,6-dione

C16H15NO3S

PRODUCTS

生成物

1
结构：CC(C)OCC(O)CN1CCC2(CC1)CSC1=C(O2)c2ccccc2C(=O)C1=O
HCID57661952

未命名化合物

PROCEDURE

实验过程

Compound 169 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 2-(isopropoxymethyl)oxirane and conditions outlined in procedure X. M.p.=97-99° C.; 400 MHz 1H NMR (DMSO-d6) δ: 7.95-7.9 (m, 1H), 7.94-7.7 (m, 2H), 7.65-7.5 (m, 1H), 4.42 (br. s, 1H), 3.72 (br. s, 1H), 3.6-3.45 (m, 1H), 3.35-3.2 (m, 2H), 3.07 (s, 2H), 2.8 (m, 2H), 2.5-2.2 (m, 4H), 2.05-1.7 (m, 4H), 1.07 (d, J=5.2 Hz, 6H); LCMS: 418 [M+H].