Benzyl glycidyl ether → HCID 57661904, compound

HRID 1665368Notes

Reaction equation

HRID 1665368 reaction equation
[NH:1]1[CH2:6][CH2:5][C:4]2([O:11][C:10]3[C:12]4[C:17]([C:18](=[O:21])[C:19](=[O:20])[C:9]=3[S:8][CH2:7]2)=[CH:16][CH:15]=[CH:14][CH:13]=4)[CH2:3][CH2:2]1.[CH2:22]([O:29][CH2:30][CH:31]1[CH2:33][O:32]1)[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[CH2:22]([O:29][CH2:30][CH:31]([OH:32])[CH2:33][N:1]1[CH2:2][CH2:3][C:4]2([O:11][C:10]3[C:12]4[C:17]([C:18](=[O:21])[C:19](=[O:20])[C:9]=3[S:8][CH2:7]2)=[CH:16][CH:15]=[CH:14][CH:13]=4)[CH2:5][CH2:6]1)[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

Participants

3

Reactant 2

HCID 94247Benzyl glycidyl etherHCID 57661820Spiro[naphtho[1,2-b][1,4]oxathiine-2,4'-piperidine]-5,6-dione

Product 1

HCID 57661904HCID 57661904, compound

Procedure

Compound 171 was synthesized using spiro[naphtho[1,2-b][1,4]oxathiine-2,4′-piperidine]-5,6-dione, 2-[(benzyloxy)methyl]oxirane and conditions outlined in procedure X. LCMS: 466 [M+H]; Rt=1.01 min.

Sources & evidence

ORD record
ord-0a5ddafdb32c4cec8c9c1e5e1c2a71bc
Source dataset
uspto-grants-2011_10
Patent number
US08039503B2

Reaction notes

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