Ethyl isocyanate → HCID 44514481, compound

HRID 1665463Notes

Reaction equation

HRID 1665463 reaction equation
[N:1]1([C:7]2[N:12]=[C:11]([N:13]3[CH2:18][CH2:17][O:16][CH2:15][CH2:14]3)[N:10]=[C:9]([C:19]3[CH:25]=[CH:24][C:22]([NH2:23])=[CH:21][CH:20]=3)[N:8]=2)[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[CH2:26]([N:28]=[C:29]=[O:30])[CH3:27]>>[N:1]1([C:7]2[N:12]=[C:11]([N:13]3[CH2:18][CH2:17][O:16][CH2:15][CH2:14]3)[N:10]=[C:9]([C:19]3[CH:25]=[CH:24][C:22]([NH:23][C:29]([NH:28][CH2:26][CH3:27])=[O:30])=[CH:21][CH:20]=3)[N:8]=2)[CH2:2][CH2:3][O:4][CH2:5][CH2:6]1

Participants

3

Reactant 2

HCID 8022Ethyl isocyanateHCID 453790874-(4,6-Dimorpholino-1,3,5-triazin-2-yl)aniline

Product 1

HCID 44514481HCID 44514481, compound

Procedure

Starting from 4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)aniline (0.130 g 0.38 mmoles) and ethyl isocyanate (260 mg, 10 fold excess) the title compound was isolated as a white solid. Yield; 38 mg (25%); (M+H)=414.4

Sources & evidence

ORD record
ord-7e091fb303f34f59a36361cf5945e4e7
Source dataset
uspto-grants-2011_10
Patent number
US08039469B2

Reaction notes

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