HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22063488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 22063456 | HCID 22063456 | — |
| Reactant | 1-(4-Fluoro-3-methylphenyl)-2-methylpropan-2-amine | HCID 22063476 | — |
| Product | HCID 22063488 | HCID 22063488 | — |
Reaction Steps
1.10 g (3.1 mmol) of benzyloxy-8-(2-ethoxy-2-hydroxyacetyl)-4H-benzo[1,4]oxazin-3-one and 0.50 g (2.8 mmol) of 2-(4-fluoro-3-methylphenyl)-1,1-dimethylethylamine are reacted and worked up analogously to the method for Example 8(d). White solid. Yield: 0.75 g (47%, hydrochloride); melting point 228° C.-230° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08044046B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-3852656f114841fab824f28a4333afcb |
| Source note | uspto-grants-2011_10 |