反应详情

温度

150 °C

1-Benzyloxy-3-bromomethyl-benzene (4.95 g, 17.9 mmol) was treated with triethyl phosphite (3.2 mL, 18.7 mmol) and heated to 150° C. After 3 hours the reaction was cooled to room temperature and concentrated to give the title compound which was used without further purification (5.9 g).

1. temperatureAfter 3 hours the reaction was cooled to room temperature
2. concentrationconcentrated