HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 101043017, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | Methyl 2-amino-5-chlorobenzoate | HCID 78878 | — |
| Product | HCID 101043017 | HCID 101043017 | — |
Reaction Steps
To a solution of methyl 2-amino-5-chlorobenzoate (2.5 g) in DMF (25 mL) was added chloroacetyl chloride (1.4 mL) with ice cooling. The resulting white crystals were collected by filtration and washed with water. The resulting white crystals were dried to obtain methyl 5-chloro-2-(2-chloroacetamide)benzoate (5.4 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08044068B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-09bada62998e4c4dab64f0e3f53da79d |
| Source note | uspto-grants-2011_10 |