Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dibenzofuran | HCID 568 | — |
| Reactant | Nitric Acid | HCID 944 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 3-Nitrodibenzofuran | HCID 72897 | — |
Reaction Steps
Combine dibenzofurane (20.0 g, 0.11 mol) and acetic acid (80 ml). Heat to 65° C. Add 98% nitric acid (20.0 g, 11.8 mol). After 3 hours, cool to room temperature to give a solid. Collect the solid by filtration, rinse with water, and dry to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08044090B2 |
|---|
| Source dataset | uspto-grants-2011_10 |
|---|
| ORD ID | ord-65c9d18dcd1e4b979d097492ee7e69f4 |
|---|
| Source note | uspto-grants-2011_10 |
|---|
