Oxalic Acid → HCID 21071591, compound

HRID 1666833Notes

Reaction equation

[C:1]1(C)[CH:6]=[CH:5][CH:4]=[C:3]([O:7][C:8]2[CH:19]=[C:18]3[C:11]([NH:12][CH:13]=[C:14]3[CH2:15][CH2:16][NH2:17])=[CH:10][CH:9]=2)[CH:2]=1.[O:21]=[C:22]([C:24](=[O:26])[OH:25])[OH:23]>>[C:24]([OH:26])(=[O:25])[C:22]([OH:23])=[O:21].[O:7]([C:8]1[CH:19]=[C:18]2[C:11]([NH:12][CH:13]=[C:14]2[CH2:15][CH2:16][NH2:17])=[CH:10][CH:9]=1)[C:3]1[CH:4]=[CH:5][CH:6]=[CH:1][CH:2]=1

Participants

Reactant 2

HCID 971Oxalic Acid

HCID 21071585HCID 21071585, compound

Product 1

HCID 21071591HCID 21071591, compound

Procedure

5-m-Tolyloxytryptamine: m.p. 164-165° C.; 1H NMR (250 MHz, DMSO-d6) 2.26 (s, 3H), 2.89-3.07 (m, 4H), 4.52 (br, 2H), 6.68-6.72 (m, 2H), 6.82-6.86 (m, 2H), 7.17-7.42 (m, 4H), 11.06 (br, 1H); MS (ELECTROSPRAY) m/e: 265.1 (M−1-C2H2O4).

Sources & evidence

ORD record: ord-7df600f616884bb1b6833292daa0b677
Source dataset: uspto-grants-2011_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08044090B2

Reaction notes

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