돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1666932생성일: 2026년 10월 25일

5-Methyl-2-((2-nitrophenyl)amino)-3-thiophenecarbonitrile → 2-(2-Aminoanilino)-5-methylthiophene-3-carbonitrile

https://huagongshe.com/reaction/1666932

반응식

참여 물질

역할이름HCID투입량
반응물5-Methyl-2-((2-nitrophenyl)amino)-3-thiophenecarbonitrileHCID 395460—
촉매PalladiumHCID 23938—
용매Ethyl AcetateHCID 8857—
생성물2-(2-Aminoanilino)-5-methylthiophene-3-carbonitrileHCID 67445262—

반응 단계

2-(2-Nitroanilino)-5-methylthiophene-3-carbonitrile (100 g) is taken in ethyl acetate (1000 ml). The reaction mixture is then hydrogenated by 5% Pd/C (15 g) at 50-55° C. at 10-12 Kg pressure. The reaction mixture is filtered, and ethyl acetate is distilled off to get the title compound.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08044196B2
출처 데이터셋uspto-grants-2011_10
ORD IDord-302a18ee9fe34f6aa6145ec243e4ccee
출처 메모uspto-grants-2011_10