Aluminium lithium hydride → (Azepan-4-yl)methanol

HRID 1667304Notes

Reaction equation

HRID 1667304 reaction equation
O=[C:2]1[NH:8][CH2:7][CH2:6][CH:5]([C:9](OCC)=[O:10])[CH2:4][CH2:3]1.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[NH:8]1[CH2:2][CH2:3][CH2:4][CH:5]([CH2:9][OH:10])[CH2:6][CH2:7]1

Participants

3

Reactant 2

HCID 21226445Aluminium lithium hydrideHCID 23093698Ethyl 7-oxoazepane-4-carboxylate

Product 1

HCID 22594076(Azepan-4-yl)methanol

Procedure

Ethyl 7-oxoazepane-4-carboxylate was reacted in the presence of lithium aluminum hydride to produce azepan-4-ylmethanol.

Sources & evidence

ORD record
ord-8a7ac21744644511816adb7faecbb0a9
Source dataset
uspto-grants-2011_10
Patent number
US08044206B2

Reaction notes

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