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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1667968Generated: October 30, 2026

Hydroxybenzenesulfonic acid → HCID 86630643, compound

https://huagongshe.com/reaction/1667968

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxybenzenesulfonic acidHCID 15619088—
ReactantTak-593HCID 24767976—
SolventEthanolHCID 702—
ProductHCID 86630643HCID 8663064375%

Reaction Steps

Using N-[5-({2-[(cyclopropylcarbonyl)amino]imidazo[1,2-b]pyridazin-6-yl}oxy)-2-methylphenyl]-1,3-dimethyl-1H-pyrazole-5-carboxamide (2.00 g, 4.49 mmol), ethanol (100 mL) and benzenesulfonic acid monohydrate (0.83 g, 4.71 mmol), and in the same manner as in Example 152, the title compound (2.02 g, 75%) was obtained as white crystals.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08044049B2
Source datasetuspto-grants-2011_10
ORD IDord-bab61ee4066a4651a5a75fdb553b1677
Source noteuspto-grants-2011_10