Cyclopropanecarbonyl chloride → 2-Cyclopropyl-6,7,8,9-tetrahydro-5H-[1,3]oxazolo[4,5-h][3]benzazepine hydrochloride

Participants

Reaction Steps

The title compound was prepared in analogy to General Procedure 2 from 1,1-dimethylethyl 7-amino-8-hydroxy-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate (Preparation 9, 2.16 mmol) and cyclopropanecarbonyl chloride (2.4 mmol) to give the title compound (1.75 mmol) as a white solid.

Provenance & Evidence