3-acetyl-7-nitro-2,3,4,5-tetrahydro-1H-benzo[d]azepine → HCID 21822924, compound

Participants

Reaction Steps

To a solution of 1-(7-nitro-1,2,4,5-tetrahydrobenzo[d]azepin-3-yl)ethanone (4.0 g) in ethanol (120 ml) 10% Pd/C was added (150 mg) and the mixture hydrogenated for 1 h under a pressure of 30 psi of H2. The mixture was filtered through a celite pad and concentrated to afford a white solid (3.15 g, 90% yield).

Provenance & Evidence