HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 57825156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Acetonitrile ethyl acetate | HCID 21930812 | — |
| Reactant | HCID 57825153 | HCID 57825153 | — |
| Catalyst | HCID 178513473 | HCID 178513473 | — |
| Product | HCID 57825156 | HCID 57825156 | 55% |
Reaction Steps
mixture of 4-[1-(3-bromo-phenyl)-vinyl]-1-isopropoxy-2-methyl-benzene (6.8, 20.5 mmol) and silver cyanate in ethyl acetate/acetonitrile. The crude product of this reaction was subsequently reacted with aqueous ammonia (30% by vol). Purification by SCX column yielded 4.3 g of product (55%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989449B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-ad07d921db974dfa80eb638e3667c540 |
| Source note | uspto-grants-2011_08 |