HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzamide → HCID 178489011, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzamide | HCID 2331 | — |
| Reactant | p-Anisoyl chloride | HCID 7477 | — |
| Reactant | 2-Amino-4-methoxy-3-methylbenzamide | HCID 59165435 | — |
| Product | HCID 178489011 | HCID 178489011 | 92% |
Reaction Steps
The general procedure described in Example 31 was followed using 2-amino-4-methoxy-3-methyl benzamide as benzamide derivative [A] and 4-methoxybenzoic acid chloride as acid chloride [B], which gave the title compound (5.5 g, 92%). 1H-NMR DMSO-D6 δ 2.38 (s, 3H), 3.82 (s, 3H), 3.92 (s, 3H), 7.04 (d, 2H), 7.20 (d, 1H), 8.00 (d, 1H), 8.20 (d, 2H), 12.18 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989471B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-0ffe5bb89bb644e0a8ce27d2722cf918 |
| Source note | uspto-grants-2011_08 |