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HRID 1670068作成日:2026年10月25日

3-Methoxy-5-nitrobenzoic acid → 3-Amino-5-methoxybenzoic acid

https://huagongshe.com/reaction/1670068

反応式

関与物質

役割名称HCID仕込み量
反応物3-Methoxy-5-nitrobenzoic acidHCID 5300212—
溶媒EthanolHCID 702—
生成物3-Amino-5-methoxybenzoic acidHCID 13874409111%

反応手順

3-Methoxy-5-nitrobenzoic acid (510 mg) was dissolved in 5 ml of ethanol and 10% Pd(C) (50 mg) was added. The resulting suspension was stirred under a hydrogen-filled balloon for 2 hours. Then the reaction mixture was filtered and concentrated to dryness. Isolated dark brown solid (480 mg) was used without further purification in the next step.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07989454B2
出典データセットuspto-grants-2011_08
ORD IDord-76d3b3a100064435bd6b6c4a24bb7ea5
出典メモuspto-grants-2011_08