化工社化工社 化学情報印刷レポート · 研究参考用
3-Methoxy-5-nitrobenzoic acid → 3-Amino-5-methoxybenzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Methoxy-5-nitrobenzoic acid | HCID 5300212 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 3-Amino-5-methoxybenzoic acid | HCID 13874409 | 111% |
反応手順
3-Methoxy-5-nitrobenzoic acid (510 mg) was dissolved in 5 ml of ethanol and 10% Pd(C) (50 mg) was added. The resulting suspension was stirred under a hydrogen-filled balloon for 2 hours. Then the reaction mixture was filtered and concentrated to dryness. Isolated dark brown solid (480 mg) was used without further purification in the next step.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07989454B2 |
| 出典データセット | uspto-grants-2011_08 |
| ORD ID | ord-76d3b3a100064435bd6b6c4a24bb7ea5 |
| 出典メモ | uspto-grants-2011_08 |