HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-fluorophenylboronic Acid → HCID 67340031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-fluorophenylboronic Acid | HCID 2778656 | — |
| Reactant | HCID 67338116 | HCID 67338116 | — |
| Product | HCID 67340031 | HCID 67340031 | 40% |
Reaction Steps
The title compound was prepared according to the general procedure described in Steps 3 and 4 of Method F starting from 4-[3-[6-(3-bromo-5-dimethylcarbamoyl-phenoxy)-hexyl]-2-(2-ethoxycarbonyl-ethyl)-phenoxy]-butyric acid ethyl ester and 4-chloro-3-fluorophenylboronic acid. LC/MS indicated a purity of 92% as measured by UV 214 nM. Yield: 40% (after two steps)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07989454B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-3d4c125ef6804e44a176c2a252e09b1a |
| Source note | uspto-grants-2011_08 |