12-Bromo-1-dodecanol → HCID 20527985, compound

HRID 1670380Notes

Reaction equation

HRID 1670380 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][OH:14].[CH3:15][CH:16]([CH3:22])[CH2:17][CH2:18][CH2:19][CH2:20]Br>>[CH3:15][CH:16]([CH3:22])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][OH:14]

Participants

3

Reactant 2

HCID 13789512-Bromo-1-dodecanolHCID 5207261-Bromo-5-methylhexane

Product 1

HCID 20527985HCID 20527985, compoundYield 44%

Procedure

17-methyloctadecan-1-ol was prepared from 12-bromo-1-dodecanol and 5-methylhexylbromide in 44% yield. 1H NMR δ 0.86 (6H), 1.10-1.40 (32H), 3.64 (2H).

Sources & evidence

ORD record
ord-1c57740e81914f32b97f9f5b7daaa300
Source dataset
uspto-grants-2011_08
Patent number
US07994143B2

Reaction notes

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