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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1670666Generated: October 31, 2026

p-Toluenesulfonyl azide → HCID 76698471, compound

https://huagongshe.com/reaction/1670666

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Toluenesulfonyl azideHCID 13661—
ReactantEthyl 3-oxovalerateHCID 78656—
ProductHCID 76698471HCID 76698471—

Reaction Steps

This compound was synthesised from ethyl propionylacetate (CAS 4949-44-4) and polymer-bound tosylazide using similar protocol as described in Intermediate 1-7. Crude material (0.9 g, 95%) was taken directly to next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07994179B2
Source datasetuspto-grants-2011_08
ORD IDord-4dcba333b83a4b2284897dd5044d311e
Source noteuspto-grants-2011_08