HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59381267, compound → HCID 59381264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59381267 | HCID 59381267 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | HCID 59381264 | HCID 59381264 | 75.3% |
Reaction Steps
Preparation can be carried out analogously to Example 1 using 2.84 g (4.59 mmol) 6-({4-[(1E)-3-methoxy-3-oxoprop-1-enyl]benzoyl}oxy)hexyl 2-(4-nitrobenzyl)-3-(4-nitrophenyl)propanoate, 7.44 g (27.52 mmol) Ferric chloride hexahydrate and 3.00 g (45.89 mmol) Zinc powder yielded 1.93 g (72%) 6-({4 -[(1E)-3-methoxy-3-oxoprop-1-enyl]benzoyl}oxy)hexyl 2-(4-aminobenzyl)-3-(4 -aminophenyl)propanoate as yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07994273B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-75bc43e118a749889913a0e1f6db1123 |
| Source note | uspto-grants-2011_08 |