HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67292500, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67292943 | HCID 67292943 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67292500 | HCID 67292500 | — |
Reaction Steps
To a mixture of tert-butyl 1-(pyridazin-4-yl)cyclopropylcarbamate (0.100 g, 0.425 mmol, 1.0 eq) in a solution of 4.0 M HCl in 1,4-dioxane (4.0 ml) was stirred at r.t. for 5 hr. The reaction mixture was concentrated under vacuum and dried HCl salt was taken to next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07994171B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-b34b9ee9fbbc46aebf0da5113b958706 |
| Source note | uspto-grants-2011_08 |