HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1672108Generated: October 25, 2026
Acetic Anhydride → 2-Methyl-4-oxatricyclo[5.2.1.02,6]decan-3-yl acetate
https://huagongshe.com/reaction/1672108
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 2-Methyl-4-oxatricyclo[5.2.1.02,6]-decan-3-ol | HCID 59602256 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2-Methyl-4-oxatricyclo[5.2.1.02,6]decan-3-yl acetate | HCID 66930811 | 96% |
Reaction Steps
A mixture of 63 g of 2-methyl-4-oxatricyclo[5.2.1.02,6]decan-3-ol, 42 g of pyridine, and 51 g of acetic anhydride was heated at 50° C. for 5 hours. The reaction mixture was concentrated. The concentrate was purified by distillation, obtaining 74 g (yield 96%) of the target compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07998657B2 |
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| Source dataset | uspto-grants-2011_08 |
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| ORD ID | ord-5307b4e568854ce395de410c68e6b83d |
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| Source note | uspto-grants-2011_08 |
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