참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 4-Oxatricyclo[4.2.1.03,7]nonan-5-ol | HCID 15195820 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 4-Oxatricyclo[4.2.1.03,7]non-5-yl acetate | HCID 58143072 | 88% |
반응 단계
A mixture of 14 g of 4-oxatricyclo[4.2.1.03,7]nonan-5-ol, 12 g of pyridine and 14 g of acetic anhydride was heated at 50° C. for 5 hours. The reaction mixture was concentrated. The concentrate was purified by distillation, obtaining 16 g (yield 88%) of the target compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07998657B2 |
|---|
| 출처 데이터셋 | uspto-grants-2011_08 |
|---|
| ORD ID | ord-f4ec8b1fab2443a18c980a4ddfedae23 |
|---|
| 출처 메모 | uspto-grants-2011_08 |
|---|
