HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfanylsilane → Sulfanylsilane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfanylsilane | HCID 139670 | — |
| Reactant | Chdmdve | HCID 21867826 | — |
| Product | Sulfanylsilane | HCID 139670 | — |
| Product | Cyclohexane, 1,4-bis[(ethenyloxy)methyl]- | HCID 3437285 | — |
Reaction Steps
Mercaptosilane (SI263 made by Degussa) in 196.4 g (1 mole) and cyclohexane dimethanol divinyl ether (CHDVE made by Nippon Carbide Industries) in 98.2 g (0.5 mole) were reacted in the presence of a phosphoric acid ester catalyst at room temperature for 3 hours to obtain a blocked mercaptosilane (SI263/CHDVE) shown by the following formula:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07737203B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-51158a52a5f44e5fa67200417cae30f4 |
| Source note | uspto-grants-2010_06 |