HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroaniline → HCID 60046939, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroaniline | HCID 7240 | — |
| Reactant | HCID 60046942 | HCID 60046942 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 60046939 | HCID 60046939 | — |
Reaction Steps
The title compound is prepared in analogy to Example 19d starting from 0.7 g (2.957 mmol) of 4-chloro-6-ethyl-3-nitro-quinoline (Example 49e) and 0.37 g (3.55 mmol) 2-chloroaniline in 3 ml acetic acid. Crystallization from ethyl acetate-hexane. mp: 134-136° C.; MS: 328 (M++1); HPLC: tret=10.61 min (Grad 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07998972B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-b7e7f968a76f4771806e58d9b2f4bf89 |
| Source note | uspto-grants-2011_08 |