Ethanol → HCID 86615729, compound
Reaction equation
O.O.O.O.O.O.[Cl-].[Sr+2:8].[Cl-].[CH2:10]([S:18]([O-:21])(=[O:20])=[O:19])[CH2:11][CH2:12][CH2:13][S:14]([O-:17])(=[O:16])=[O:15].[Na+].[Na+].C(O)C>O>[CH2:10]([S:18]([O-:21])(=[O:20])=[O:19])[CH2:11][CH2:12][CH2:13][S:14]([O-:17])(=[O:15])=[O:16].[Sr+2:8]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Procedure
0.75 mol of strontium chloride hexahydrate and 0.75 mol of disodium 1,4-butane-disulphonate are dissolved in 600 ml of water. After stirring for 1 hour, 1 litre of 96% ethanol is added. The precipitate formed is filtered off, rinsed with 500 ml of a 70/30 ethanol/water mixture and dried to yield the expected product.
Workup
- customThe precipitate formed
- filtrationis filtered off
- washrinsed with 500 ml of a 70/30 ethanol/water mixture
- customdried
Sources & evidence
- ORD record
- ord-73cf63cc9c214566be3edaba93c07fa1
- Source dataset
- uspto-grants-2011_08
- Patent number
- US07999009B2
Reaction notes
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