Triethylamine → HCID 67329693, compound

Participants

Reaction Steps

To a solution of the product of Step A (100 mg, 0.22 mmol) in 5.0 mL of CH2Cl2 was added pivaloyl chloride (32 μL, 0.26 mmol) and NEt3 (46 μL, 0.33 mmol). After stirring at rt for 16 h, the reaction mixture was concentrated. Chromatography on a Biotage 25+M cartridge using 1:1 v/v EtOAc/hexanes as the eluant afforded the product as a white solid.

Provenance & Evidence