HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 57879509, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Tert-butyl 2-(benzamido)-4-(3-phenylpropyl)benzoate | HCID 67343836 | — |
| Product | HCID 57879509 | HCID 57879509 | 48.2% |
Reaction Steps
4.8 mL of trifluoroacetic acid solution containing 0.48 g of tert-butyl 2-(benzamido)-4-(3-phenylpropyl)benzoate was stirred at room temperature for 2 hours. The solvent was evaporated under reduced pressure, and the obtained residue was purified with silica gel column chromatography [eluent; hexane; ethyl acetate=1:1] to obtain 0.20 g of 2-(benzamido)-4-(3-phenylpropyl)benzoic acid as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999132B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-5752a4638f284d3d8e0eb171195e2f1a |
| Source note | uspto-grants-2011_08 |