HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67341883, compound → HCID 57879589, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67341883 | HCID 67341883 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 57879589 | HCID 57879589 | — |
Reaction Steps
10 mL of trifluoroacetic acid was added to the obtained tert-butyl 4-(3-chlorophenyl)-2-(2,3-dimethylbenzamido)benzoate and stirred at room temperature for 2 hours. The solvent was evaporated under reduced pressure and methanol was added to the obtained residue and a solid substance was separated by filtration to obtain 32 mg of 4-(3-chlorophenyl)-2-(2,3-dimethylbenzamido)benzoic acid as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999132B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-692af0ce919f48498860754942e17889 |
| Source note | uspto-grants-2011_08 |