HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 2-(benzamido)-4-(3-chlorophenyl)benzoate → 2-(Benzamido)-4-(3-chlorophenyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 2-(benzamido)-4-(3-chlorophenyl)benzoate | HCID 67344272 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | 2-(Benzamido)-4-(3-chlorophenyl)benzoic acid | HCID 57879379 | — |
Reaction Steps
10 mL of trifluoroacetic acid was added to the obtained tert-butyl 2-(benzamido)-4-(3-chlorophenyl)benzoate and stirred at room temperature for 1 hour. The solvent was evaporated under reduced pressure and methanol was added to the obtained residue and a solid substance was separated by filtration to obtain 21 mg of 2-(benzamido)-4-(3-chlorophenyl)benzoic acid as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999132B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-e92718cd844f461a989355a4478175e1 |
| Source note | uspto-grants-2011_08 |