1-Benzyl-1,4-diazepane → HCID 67340225, compound

HRID 1674774Notes

Reaction equation

HRID 1674774 reaction equation
[CH2:1]([N:8]1[CH2:14][CH2:13][CH2:12][NH:11][CH2:10][CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[C:16]1[CH:17]=[CH:18][C:19]2[N:20]([C:22]([S:25][CH3:26])=[N:23][N:24]=2)[N:21]=1>>[CH2:1]([N:8]1[CH2:14][CH2:13][CH2:12][N:11]([C:16]2[CH:17]=[CH:18][C:19]3[N:20]([C:22]([S:25][CH3:26])=[N:23][N:24]=3)[N:21]=2)[CH2:10][CH2:9]1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 2283651-Benzyl-1,4-diazepaneHCID 12893351HCID 12893351, compound

Product 1

HCID 67340225HCID 67340225, compound

Procedure

A mixture of 1-benzyl-1,4-diazepane and 6-chloro-3-methylsulfanyl-1,2,4-triazolo[4,3-b]pyridazine was allowed to react by General Synthetic Method 2 to give 6-(4-benzyl-1,4-diazepan-1-yl)-3-methylsulfanyl-[1,2,4]triazolo[4,3-b]pyridazine.

Workup

  1. customto react by General Synthetic Method 2

Sources & evidence

ORD record
ord-24c48cafc1c545618068a5961b6c2e70
Source dataset
uspto-grants-2011_08
Patent number
US08003649B2

Reaction notes

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