HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Chloro-3-(trifluoromethoxy)phenyl)methanol → 4-Chloro-3-(trifluoromethoxy)benzyl bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Chloro-3-(trifluoromethoxy)phenyl)methanol | HCID 17750696 | — |
| Reactant | 2-Bromo-4-(bromomethyl)-1-(trifluoromethoxy)benzene | HCID 59300671 | — |
| Product | 4-Chloro-3-(trifluoromethoxy)benzyl bromide | HCID 17750697 | — |
Reaction Steps
Compound 35.2 was synthesized from (4-chloro-3-(trifluoromethoxy)phenyl)-methanol using the procedure described for the preparation of 19.2. 1H NMR (500 MHz, DMSO-d6) δ 7.74 (1 H, d, J=2.0 Hz), 7.38-7.53 (2 H, m), 4.53 (2 H, d, J=5.6 Hz)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003648B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-40c0225e8a9648c797f3a2da478fc80a |
| Source note | uspto-grants-2011_08 |