7-Bromo-1-heptene → n-Methylhept-5-en-1-amine tosylate salt

HRID 1675392Notes

Reaction equation

HRID 1675392 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH:7]=[CH2:8].[S:9]([C:13]1[CH:19]=[CH:18][C:16]([CH3:17])=[CH:15][CH:14]=1)([OH:12])(=[O:11])=[O:10].[CH3:20][NH:21]CCCCC=C>>[S:9]([C:13]1[CH:19]=[CH:18][C:16]([CH3:17])=[CH:15][CH:14]=1)([OH:12])(=[O:11])=[O:10].[CH3:20][NH:21][CH2:2][CH2:3][CH2:4][CH2:5][CH:6]=[CH:7][CH3:8]

Participants

3

Reactant 2

HCID 5244507-Bromo-1-hepteneHCID 46737741N-methylhex-5-en-1-amine 4-methylbenzenesulfonate

Product 1

HCID 131729112n-Methylhept-5-en-1-amine tosylate salt

Procedure

Compound 32b was synthesized from 7-bromo-heptene as a white solid in quantitative yield, following the procedure as described for compound 32a.

Sources & evidence

ORD record
ord-3a70618ade8e41168f56e541af926396
Source dataset
uspto-grants-2011_08
Patent number
US08003659B2

Reaction notes

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