HuagongsheHuagongshe Chemistry Print Report · For research reference only
(S)-tert-butyl-5-(nitrooxy)hexanoate → (S)-5-(nitrooxy)hexanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (S)-tert-butyl-5-(nitrooxy)hexanoate | HCID 58231672 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | (S)-5-(nitrooxy)hexanoic acid | HCID 58231663 | — |
Reaction Steps
(S)-tert-butyl-5-(nitrooxy)hexanoate (590 mg, 2.53 mmol), was dissolved in CH2Cl2 (20 mL). HClgas was bubbled into the solution until the disappearance of the starting material. The solution was reduced to a small volume and diluted in CH2Cl2 few times to remove residual acidity, then used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003811B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-484fde50b49a4e15a7d1d02cdd4e4e35 |
| Source note | uspto-grants-2011_08 |