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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1676022Generated: October 31, 2026

HCID 58653709, compound → HCID 58653696, compound

https://huagongshe.com/reaction/1676022

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 58653709HCID 58653709—
SolventHydrochloric AcidHCID 313—
ProductHCID 58653696HCID 58653696—

Reaction Steps

A solution of ethyl (2E)-3-(1H-benzimidazol-1-yl)-3-(4-ethylphenyl)-2-propenoate (46 mg, 143 μmol) in hydrochloric acid (10 mL of a 5N solution) was stirred at room temperature for 72 hours, and then heated at reflux for 6 hours. The solution was cooled to room temperature, and evaporated in vacuo to afford the title compound, [LCMS (Method A, Mobile Phase I) RT=6.62 min, MH+ 294].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08003806B2
Source datasetuspto-grants-2011_08
ORD IDord-eeb4580a756f4d8f9da20fd0b57e4507
Source noteuspto-grants-2011_08