HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58653709, compound → HCID 58653696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58653709 | HCID 58653709 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 58653696 | HCID 58653696 | — |
Reaction Steps
A solution of ethyl (2E)-3-(1H-benzimidazol-1-yl)-3-(4-ethylphenyl)-2-propenoate (46 mg, 143 μmol) in hydrochloric acid (10 mL of a 5N solution) was stirred at room temperature for 72 hours, and then heated at reflux for 6 hours. The solution was cooled to room temperature, and evaporated in vacuo to afford the title compound, [LCMS (Method A, Mobile Phase I) RT=6.62 min, MH+ 294].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003806B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-eeb4580a756f4d8f9da20fd0b57e4507 |
| Source note | uspto-grants-2011_08 |