HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 11591041, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | HCID 58653688 | HCID 58653688 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 11591041 | HCID 11591041 | — |
Reaction Steps
A solution of ethyl 3-{5-[(2-phenoxybenzoyl)amino]-1H-benzimidazol-1-yl}-3-phenylpropanoate (68 mg, 135 μmol) in a mixture of hydrochloric acid (20 mL of a 5N solution) and acetonitrile (20 mL) was stirred at room temperature for 48 hours. The solution was then concentrated in vacuo, and the resulting solid filtered off and vacuum-dried to afford the title compound, [LCMS (Method A, Mobile Phase I) RT=2.70 min, MH+ 478].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003806B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-d3885f6aa84f4279929659d91c64cead |
| Source note | uspto-grants-2011_08 |