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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1676055Generated: November 4, 2026

Acetonitrile → HCID 11591041, compound

https://huagongshe.com/reaction/1676055

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetonitrileHCID 6342—
ReactantHCID 58653688HCID 58653688—
SolventHydrochloric AcidHCID 313—
ProductHCID 11591041HCID 11591041—

Reaction Steps

A solution of ethyl 3-{5-[(2-phenoxybenzoyl)amino]-1H-benzimidazol-1-yl}-3-phenylpropanoate (68 mg, 135 μmol) in a mixture of hydrochloric acid (20 mL of a 5N solution) and acetonitrile (20 mL) was stirred at room temperature for 48 hours. The solution was then concentrated in vacuo, and the resulting solid filtered off and vacuum-dried to afford the title compound, [LCMS (Method A, Mobile Phase I) RT=2.70 min, MH+ 478].

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08003806B2
Source datasetuspto-grants-2011_08
ORD IDord-d3885f6aa84f4279929659d91c64cead
Source noteuspto-grants-2011_08