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HRID1676082

反应详情

EQUATION

反应方程式

HRID 1676082 的结构方程式

REACTANTS

反应物

3
结构：O=[N+]([O-])c1ccc(Cl)c([N+](=O)[O-])c1
HCID6

1-Chloro-2,4-Dinitrobenzene

C6H3ClN2O4

结构：COC(=O)C[C@H](N)c1ccccc1
HCID788099

methyl (3S)-3-amino-3-phenylpropanoate

C10H13NO2

结构：Nc1ccccc1C(=O)Nc1ccc2ncn(C(CC(=O)O)c3ccccc3)c2c1
HCID11611040

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O)C[C@@H](c1ccccc1)n1cnc2cc([N+](=O)[O-])ccc21
HCID58653644

未命名化合物

PROCEDURE

实验过程

Using a similar procedure to that described in Preparation 45, the title compound (19 mg) was prepared from methyl (3S)-3-amino-3-phenylpropanoate and 2,4-dinitrochlorobenzene, and liberated as the free acid using a procedure similar to that described in Preparation II. [LCMS (Method C, Mobile Phase I) RT=2.60 min, MH+ 312].

WORKUP

后处理

  1. customthat described in Preparation 45