Ethylene Glycol → HCID 24772640, compound

HRID 1676850Notes

Reaction equation

HRID 1676850 reaction equation
[CH3:1][O:2][C:3]([CH2:5][O:6][C:7](=[O:17])[C:8]1[CH:13]=[CH:12][C:11]([N:14]=[C:15]=[O:16])=[CH:10][CH:9]=1)=[O:4].[CH2:18]([OH:21])[CH2:19][OH:20]>O>[CH3:1][O:2][C:3]([CH2:5][O:6][C:7](=[O:17])[C:8]1[CH:13]=[CH:12][C:11]([NH:14][C:15]([O:20][CH2:19][CH2:18][OH:21])=[O:16])=[CH:10][CH:9]=1)=[O:4]

Participants

4

Reactant 2

HCID 174Ethylene GlycolHCID 58894692HCID 58894692, compound

Product 1

HCID 24772640HCID 24772640, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

4-Isocyanato-benzoic acid methoxycarbonylmethyl ester 9 (5 grams, 21.09 mmol) is added to ethylene glycol (20 mL) at room temperature and stirred for 6 hours. Water (100 mL) is added, and crude 10 is filtered, dried, and purified by a suitable method.

Workup

  1. filtrationcrude 10 is filtered
  2. customdried
  3. custompurified by a suitable method

Sources & evidence

ORD record
ord-d8590f55302f4c19bb10af7411b314a4
Source dataset
uspto-grants-2011_08
Patent number
US08007526B2

Reaction notes

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