HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piretanide → HCID 11575958, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piretanide | HCID 4849 | — |
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(Dimethylamino)propyl chloride hydrochloride | HCID 94308 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 11575958 | HCID 11575958 | — |
Reaction Steps
In a similar manner to Example 31, piretanide can be reacted with 3-(dimethylamino)propyl chloride hydrochloride, triethylamine and sodium iodide in dimethylformamide (DMF) to yield 3-(N,N-dimethylaminopropyl 3-aminosulfonyl-4-phenoxy-5-(1-pyrrolidinyl)benzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008283B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-24ff1b0503714307a7845621ef601430 |
| Source note | uspto-grants-2011_08 |