HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzaldehyde → HCID 67374585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 67373781 | HCID 67373781 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67374585 | HCID 67374585 | — |
Reaction Steps
The product from Example 89, Step A was combined with 1.2 equivalents of 4-methoxybenzaldehyde and 1.5 equivalent of sodium triacetoxyborohydride in dichloroethane. The reaction was stirred for 1.5 hours at room temperature, was diluted with EtOAc and washed with sat. NaHCO3 and brine. The solution was dried with Na2SO4 and concentrated in vacuo to give the titled compound. ESI+ MS: 651 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008295B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-0d07fe84772b4ba3891f5c48f759cac5 |
| Source note | uspto-grants-2011_08 |