HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 1-Methyl-cycloheptanecarbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1-Methylcycloheptane-1-carboxylic acid | HCID 12757489 | — |
| Product | 1-Methyl-cycloheptanecarbonyl chloride | HCID 21535496 | 99% |
Reaction Steps
A solution of 1-methyl-cycloheptanecarboxylic acid (156 mg, 0.998 mmol) (Journal of Organic Chemistry (1982), 47(17), 3242-7) in thionyl chloride (5 ml) was stirred at room temperature for 2 days and then concentrated on high vacuum giving 174 mg (99%) of 1-methyl-cycloheptanecarbonyl chloride as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08008298B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-43cd66044f5f4b11b68e96d62e7621d2 |
| Source note | uspto-grants-2011_08 |